• Instructor Homepages

Introduction Materials (note, current versions of some of the following materials are available only in eLearn)

• Getting Started
• Course Overview and First Day Notes
• MSDS: Material Data Safety Sheets
• Recommended First Aid Procedures
• Example of Write Up
• Examples of Glassware
• Laboratory Safety Procedures Agreement
• Apparatus List
• Tutorials, Chemical properties, spectroscopy, NFPA Hazard Labels
• SuperOrganicLab, information on laboratory techniques and instruments

Experiment A: Separation of an organic acid from a mixture

• Experiment A Directions
• Experiment A Notes

Videos

• Background and Theory RealPlayer Word Document
• Weighing RealPlayer
• Dissolving Sample RealPlayer
• Filtration RealPlayer
• Extraction RealPlayer
• Precipitation RealPlayer

Experiment B: Chromatographic Separation of Organic Compounds

• Experiment B Directions
• Experiment B Notes

Videos

• Theory and Background Real Player
• Thin layer Chromatography RealPlayer

Experiment C: Separation of Panacetin Components

• Experiment C Notes

Videos

• Theory and Background RealPlayer
• Evaporation RealPlayer

Experiment D: Recrystallization and Identification of Unknown

• Experiment D Notes

Videos

• Theory and Background RealPlayer
• Recrystallization RealPlayer
• Vacuum Filtration RealPlayer
• Melting Point Determination RealPlayer

Experiment E: Nucleophilic Substitution

• Experiment E Directions
• Experiment E Notes

Videos

• Positive and negative test with NaI/Acetone
• Positive and negative test with Lucas's reagent (ZnCl₂/HCl)
• Positive and negative test with AgNO₃

Experiment F: Addition of Bromination to Cinnamic Acid

• Experiment F Notes

Experiment G: Separation of Alcohols by Fractional Distillation

• Experiment G Directions
• Experiment G Notes

Videos

• Theory and Background
  • Distillation RealPlayer
  • HETP RealPlayer and Notes
• Fractional Distillation RealPlayer
• Gas Chromatography RealPlayer

Experiment I: Preparation of Camphor

• Experiment I Notes
• Experiment I 2nd week Notes

Videos

• Oxidation RealPlayer
• Sublimation RealPlayer